Design, development, and demonstration of a fully LabVIEW controlled in situ electrochemical Fourier transform infrared setup combined with a wall-jet electrode to investigate the electrochemical interface of nanoparticulate electrocatalysts under reaction conditions

Markus Nesselberger; Sean James Ashton; Gustav Karl Henrik Wiberg; Matthias Arenz

doi:10.1063/1.4816826

Design, development, and demonstration of a fully LabVIEW controlled in situ electrochemical Fourier transform infrared setup combined with a wall-jet electrode to investigate the electrochemical interface of nanoparticulate electrocatalysts under reaction conditions

Markus Nesselberger, Sean James Ashton, Gustav Karl Henrik Wiberg, Matthias Arenz

Department of Chemistry

10 Citations (Scopus)

Abstract

We present a detailed description of the construction of an in situ electrochemical ATR-FTIR setup combined with a wall-jet electrode to investigate the electrocatalytic properties of nanoparticulate catalysts in situ under controlled mass transport conditions. The presented setup allows the electrochemical interface to be probed in combination with the simultaneous determination of reaction rates. At the same time, the high level of automation allows it to be used as a standard tool in electrocatalysis research. The performance of the setup was demonstrated by probing the oxygen reduction reaction on a platinum black catalyst in sulfuric electrolyte.

Original language	English
Article number	074103
Journal	Review of Scientific Instruments
Volume	84
Number of pages	7
ISSN	0034-6748
DOIs	https://doi.org/10.1063/1.4816826
Publication status	Published - Jul 2013

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10.1063/1.4816826

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Nesselberger, M., Ashton, S. J., Wiberg, G. K. H., & Arenz, M. (2013). Design, development, and demonstration of a fully LabVIEW controlled in situ electrochemical Fourier transform infrared setup combined with a wall-jet electrode to investigate the electrochemical interface of nanoparticulate electrocatalysts under reaction conditions. Review of Scientific Instruments, 84, Article 074103. https://doi.org/10.1063/1.4816826

Design, development, and demonstration of a fully LabVIEW controlled in situ electrochemical Fourier transform infrared setup combined with a wall-jet electrode to investigate the electrochemical interface of nanoparticulate electrocatalysts under reaction conditions. / Nesselberger, Markus; Ashton, Sean James; Wiberg, Gustav Karl Henrik et al.
In: Review of Scientific Instruments, Vol. 84, 074103, 07.2013.

Research output: Contribution to journal › Journal article › Research › peer-review

Nesselberger, M, Ashton, SJ, Wiberg, GKH & Arenz, M 2013, 'Design, development, and demonstration of a fully LabVIEW controlled in situ electrochemical Fourier transform infrared setup combined with a wall-jet electrode to investigate the electrochemical interface of nanoparticulate electrocatalysts under reaction conditions', Review of Scientific Instruments, vol. 84, 074103. https://doi.org/10.1063/1.4816826

Nesselberger M, Ashton SJ, Wiberg GKH, Arenz M. Design, development, and demonstration of a fully LabVIEW controlled in situ electrochemical Fourier transform infrared setup combined with a wall-jet electrode to investigate the electrochemical interface of nanoparticulate electrocatalysts under reaction conditions. Review of Scientific Instruments. 2013 Jul;84:074103. doi: 10.1063/1.4816826

Nesselberger, Markus ; Ashton, Sean James ; Wiberg, Gustav Karl Henrik et al. / Design, development, and demonstration of a fully LabVIEW controlled in situ electrochemical Fourier transform infrared setup combined with a wall-jet electrode to investigate the electrochemical interface of nanoparticulate electrocatalysts under reaction conditions. In: Review of Scientific Instruments. 2013 ; Vol. 84.

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