Solid-phase microextraction coupled with atomic emission spectroscopy - Rapid screening for volatile chlorinated compounds

Svein Ingar Semb; Stig Pedersen-Bjergaard; Einar Magne Brevik

doi:10.1016/S0045-6535(02)00502-7

Solid-phase microextraction coupled with atomic emission spectroscopy - Rapid screening for volatile chlorinated compounds

Svein Ingar Semb^*, Stig Pedersen-Bjergaard, Einar Magne Brevik

^*Corresponding author for this work

7 Citations (Scopus)

Abstract

Solid-phase microextraction (SPME) coupled with atomic emission spectroscopy was evaluated as a rapid screening tool for volatile halogenated compounds in water samples. After extraction, the SPME fiber was introduced to the injector where the analytes were rapidly and efficiently desorbed. The analytes entered the detector over a short period of time and produced one well-defined analyte signal. Element selective responses were measured to confirm the presence and to roughly estimate the content of volatile compounds. The total time for extraction and detection was approximately 5 min, which makes this method a rapid and promising technique for determination of total amount of volatile halogenated compounds. The proposed technique may prove useful as a screening test in order to pinpoint the samples that need further assessment by capillary gas chromatography.

Original language	English
Journal	Chemosphere
Volume	49
Issue number	10
Pages (from-to)	1349-1355
Number of pages	7
ISSN	0045-6535
DOIs	https://doi.org/10.1016/S0045-6535(02)00502-7
Publication status	Published - 1 Dec 2002

Keywords

AES
Screening
SPME
Volatile halogenated compounds

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10.1016/S0045-6535(02)00502-7

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title = "Solid-phase microextraction coupled with atomic emission spectroscopy - Rapid screening for volatile chlorinated compounds",

abstract = "Solid-phase microextraction (SPME) coupled with atomic emission spectroscopy was evaluated as a rapid screening tool for volatile halogenated compounds in water samples. After extraction, the SPME fiber was introduced to the injector where the analytes were rapidly and efficiently desorbed. The analytes entered the detector over a short period of time and produced one well-defined analyte signal. Element selective responses were measured to confirm the presence and to roughly estimate the content of volatile compounds. The total time for extraction and detection was approximately 5 min, which makes this method a rapid and promising technique for determination of total amount of volatile halogenated compounds. The proposed technique may prove useful as a screening test in order to pinpoint the samples that need further assessment by capillary gas chromatography.",

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T1 - Solid-phase microextraction coupled with atomic emission spectroscopy - Rapid screening for volatile chlorinated compounds

AU - Semb, Svein Ingar

AU - Pedersen-Bjergaard, Stig

AU - Brevik, Einar Magne

PY - 2002/12/1

Y1 - 2002/12/1

N2 - Solid-phase microextraction (SPME) coupled with atomic emission spectroscopy was evaluated as a rapid screening tool for volatile halogenated compounds in water samples. After extraction, the SPME fiber was introduced to the injector where the analytes were rapidly and efficiently desorbed. The analytes entered the detector over a short period of time and produced one well-defined analyte signal. Element selective responses were measured to confirm the presence and to roughly estimate the content of volatile compounds. The total time for extraction and detection was approximately 5 min, which makes this method a rapid and promising technique for determination of total amount of volatile halogenated compounds. The proposed technique may prove useful as a screening test in order to pinpoint the samples that need further assessment by capillary gas chromatography.

AB - Solid-phase microextraction (SPME) coupled with atomic emission spectroscopy was evaluated as a rapid screening tool for volatile halogenated compounds in water samples. After extraction, the SPME fiber was introduced to the injector where the analytes were rapidly and efficiently desorbed. The analytes entered the detector over a short period of time and produced one well-defined analyte signal. Element selective responses were measured to confirm the presence and to roughly estimate the content of volatile compounds. The total time for extraction and detection was approximately 5 min, which makes this method a rapid and promising technique for determination of total amount of volatile halogenated compounds. The proposed technique may prove useful as a screening test in order to pinpoint the samples that need further assessment by capillary gas chromatography.

KW - AES

KW - Screening

KW - SPME

KW - Volatile halogenated compounds

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DO - 10.1016/S0045-6535(02)00502-7

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AN - SCOPUS:0036882524

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SP - 1349

EP - 1355

JO - Chemosphere

JF - Chemosphere

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Solid-phase microextraction coupled with atomic emission spectroscopy - Rapid screening for volatile chlorinated compounds

Abstract

Keywords

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