Sample cell for studying liquid interfaces with an in situ electric field using X-ray reflectivity and application to clay particles at oil–oil interfaces

Simon R. Larsen; Marie Hansteen; Barbara Pacakova; Keld Theodor; Thomas Arnold; Adrian R. Rennie; Geir Helgesen; Kenneth D. Knudsen; Heloisa N. Bordallo; Jon Otto Fossum; Leide P. Cavalcanti

doi:10.1107/S1600577518004848

Sample cell for studying liquid interfaces with an in situ electric field using X-ray reflectivity and application to clay particles at oil–oil interfaces

Simon R. Larsen, Marie Hansteen, Barbara Pacakova, Keld Theodor, Thomas Arnold, Adrian R. Rennie, Geir Helgesen, Kenneth D. Knudsen, Heloisa N. Bordallo, Jon Otto Fossum, Leide P. Cavalcanti

Xray and Neutron Science

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Abstract

Commissioning results of a liquid sample cell for X-ray reflectivity studies with an in situ applied electrical field are presented. The cell consists of a Plexiglas container with lateral Kapton windows for air–liquid and liquid–liquid interface studies, and was constructed with grooves to accept plate electrodes on the walls parallel to the direction of the beam. Both copper and ITO plate electrodes have been used, the latter being useful for simultaneous optical studies. Commissioning tests were made at the I07 beamline of the Diamond Light Source.

Original language	English
Journal	Journal of Synchrotron Radiation
Volume	25
Issue number	3
Pages (from-to)	915-917
ISSN	0909-0495
DOIs	https://doi.org/10.1107/S1600577518004848
Publication status	Published - 1 May 2018

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pp5114Final published version, 427 KBLicence: CC BY

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Larsen, S. R., Hansteen, M., Pacakova, B., Theodor, K., Arnold, T., Rennie, A. R., Helgesen, G., Knudsen, K. D., Bordallo, H. N., Fossum, J. O., & Cavalcanti, L. P. (2018). Sample cell for studying liquid interfaces with an in situ electric field using X-ray reflectivity and application to clay particles at oil–oil interfaces. Journal of Synchrotron Radiation, 25(3), 915-917. https://doi.org/10.1107/S1600577518004848

Sample cell for studying liquid interfaces with an in situ electric field using X-ray reflectivity and application to clay particles at oil–oil interfaces. / Larsen, Simon R.; Hansteen, Marie; Pacakova, Barbara et al.

In: Journal of Synchrotron Radiation, Vol. 25, No. 3, 01.05.2018, p. 915-917.

Research output: Contribution to journal › Journal article › Research › peer-review

Larsen, SR, Hansteen, M, Pacakova, B, Theodor, K, Arnold, T, Rennie, AR, Helgesen, G, Knudsen, KD, Bordallo, HN, Fossum, JO & Cavalcanti, LP 2018, 'Sample cell for studying liquid interfaces with an in situ electric field using X-ray reflectivity and application to clay particles at oil–oil interfaces', Journal of Synchrotron Radiation, vol. 25, no. 3, pp. 915-917. https://doi.org/10.1107/S1600577518004848

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title = "Sample cell for studying liquid interfaces with an in situ electric field using X-ray reflectivity and application to clay particles at oil–oil interfaces",

abstract = "Commissioning results of a liquid sample cell for X-ray reflectivity studies with an in situ applied electrical field are presented. The cell consists of a Plexiglas container with lateral Kapton windows for air–liquid and liquid–liquid interface studies, and was constructed with grooves to accept plate electrodes on the walls parallel to the direction of the beam. Both copper and ITO plate electrodes have been used, the latter being useful for simultaneous optical studies. Commissioning tests were made at the I07 beamline of the Diamond Light Source.",

author = "Larsen, {Simon R.} and Marie Hansteen and Barbara Pacakova and Keld Theodor and Thomas Arnold and Rennie, {Adrian R.} and Geir Helgesen and Knudsen, {Kenneth D.} and Bordallo, {Heloisa N.} and Fossum, {Jon Otto} and Cavalcanti, {Leide P.}",

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AU - Larsen, Simon R.

AU - Hansteen, Marie

AU - Pacakova, Barbara

AU - Theodor, Keld

AU - Arnold, Thomas

AU - Rennie, Adrian R.

AU - Helgesen, Geir

AU - Knudsen, Kenneth D.

AU - Bordallo, Heloisa N.

AU - Fossum, Jon Otto

AU - Cavalcanti, Leide P.

PY - 2018/5/1

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N2 - Commissioning results of a liquid sample cell for X-ray reflectivity studies with an in situ applied electrical field are presented. The cell consists of a Plexiglas container with lateral Kapton windows for air–liquid and liquid–liquid interface studies, and was constructed with grooves to accept plate electrodes on the walls parallel to the direction of the beam. Both copper and ITO plate electrodes have been used, the latter being useful for simultaneous optical studies. Commissioning tests were made at the I07 beamline of the Diamond Light Source.

AB - Commissioning results of a liquid sample cell for X-ray reflectivity studies with an in situ applied electrical field are presented. The cell consists of a Plexiglas container with lateral Kapton windows for air–liquid and liquid–liquid interface studies, and was constructed with grooves to accept plate electrodes on the walls parallel to the direction of the beam. Both copper and ITO plate electrodes have been used, the latter being useful for simultaneous optical studies. Commissioning tests were made at the I07 beamline of the Diamond Light Source.

U2 - 10.1107/S1600577518004848

DO - 10.1107/S1600577518004848

M3 - Journal article

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SN - 0909-0495

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JO - Journal of Synchrotron Radiation

JF - Journal of Synchrotron Radiation

IS - 3

ER -

Sample cell for studying liquid interfaces with an in situ electric field using X-ray reflectivity and application to clay particles at oil–oil interfaces

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