Design and test of a flexible electrochemical setup for measurements in aqueous electrolyte solutions at elevated temperature and pressure

TY - JOUR

T1 - Design and test of a flexible electrochemical setup for measurements in aqueous electrolyte solutions at elevated temperature and pressure

AU - Wiberg, Gustav Karl Henrik

AU - Fleige, Michael

AU - Arenz, Matthias

PY - 2014/8

Y1 - 2014/8

N2 - We present a detailed description of the construction and testing of an electrochemical cell allowing measurements at elevated temperature and pressure. The cell consists of a stainless steel pressure vessel containing the electrochemical glass cell exhibiting a three electrode configuration. The design of the working electrode is inspired by conventional rotating disk electrode setups. As demonstrated, the setup can be used to investigate temperature dependent electrochemical processes on polycrystalline platinum and also high surface area type electrocatalysts.

AB - We present a detailed description of the construction and testing of an electrochemical cell allowing measurements at elevated temperature and pressure. The cell consists of a stainless steel pressure vessel containing the electrochemical glass cell exhibiting a three electrode configuration. The design of the working electrode is inspired by conventional rotating disk electrode setups. As demonstrated, the setup can be used to investigate temperature dependent electrochemical processes on polycrystalline platinum and also high surface area type electrocatalysts.

U2 - 10.1063/1.4890826

DO - 10.1063/1.4890826

M3 - Journal article

C2 - 25173310

SN - 0034-6748

VL - 85

JO - Review of Scientific Instruments

JF - Review of Scientific Instruments

M1 - 085105

ER -