‘‘Perfecting’’ WATERGATE: clean proton NMR spectra from aqueous solution

Ralph W. Adams; Chloe M. Holroyd; Juan A. Aguilar; Lars Mathias Nilsson; Gareth A. Morris

doi:10.1039/c2cc37579f

‘‘Perfecting’’ WATERGATE: clean proton NMR spectra from aqueous solution

Ralph W. Adams, Chloe M. Holroyd, Juan A. Aguilar, Lars Mathias Nilsson, Gareth A. Morris

Food Analytics and Biotechnology

63 Citations (Scopus)

3 Downloads (Pure)

Abstract

A simple modification of the WATERGATE solvent suppression method greatly improves the quality of ¹H NMR spectra obtainable from samples in H₂O. The new method allows ¹H signals to be measured even when close in chemical shift to the signal of water, as for example in the NMR spectra of carbohydrates.

Original language	English
Journal	Chemical Communications
Volume	49
Issue number	4
Pages (from-to)	358-360
Number of pages	3
ISSN	1359-7345
DOIs	https://doi.org/10.1039/c2cc37579f
Publication status	Published - 2013

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“Perfecting” WATERGATE: clean proton NMR spectra from aqueous solutionFinal published version, 1.03 MB

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title = "{\textquoteleft}{\textquoteleft}Perfecting{\textquoteright}{\textquoteright} WATERGATE: clean proton NMR spectra from aqueous solution",

abstract = "A simple modification of the WATERGATE solvent suppression method greatly improves the quality of 1H NMR spectra obtainable from samples in H2O. The new method allows 1H signals to be measured even when close in chemical shift to the signal of water, as for example in the NMR spectra of carbohydrates.",

author = "Adams, {Ralph W.} and Holroyd, {Chloe M.} and Aguilar, {Juan A.} and Nilsson, {Lars Mathias} and Morris, {Gareth A.}",

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AU - Nilsson, Lars Mathias

AU - Morris, Gareth A.

PY - 2013

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N2 - A simple modification of the WATERGATE solvent suppression method greatly improves the quality of 1H NMR spectra obtainable from samples in H2O. The new method allows 1H signals to be measured even when close in chemical shift to the signal of water, as for example in the NMR spectra of carbohydrates.

AB - A simple modification of the WATERGATE solvent suppression method greatly improves the quality of 1H NMR spectra obtainable from samples in H2O. The new method allows 1H signals to be measured even when close in chemical shift to the signal of water, as for example in the NMR spectra of carbohydrates.

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DO - 10.1039/c2cc37579f

M3 - Journal article

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SN - 1359-7345

VL - 49

SP - 358

EP - 360

JO - Chemical Communications

JF - Chemical Communications

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ER -

‘‘Perfecting’’ WATERGATE: clean proton NMR spectra from aqueous solution

Abstract

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