Simultaneously Enhancing Spectral Resolution and Sensitivity in Heteronuclear Correlation NMR Spectroscopy

TY - JOUR

T1 - Simultaneously Enhancing Spectral Resolution and Sensitivity in Heteronuclear Correlation NMR Spectroscopy

AU - Paudel, Liladhar

AU - Adams, Ralph W.

AU - Kiraly, Peter

AU - Aguilar, Juan A.

AU - Foroozandeh, Mohammadali

AU - Cliff, Matthew J.

AU - Nilsson, Lars Mathias

AU - Sandor, Peter

AU - Waltho, Jonathan P.

AU - Morris, Gareth A.

PY - 2013/10/25

Y1 - 2013/10/25

N2 - BIRD's eye view: Adding periodic BIRD J-refocusing (BIRD=bilinear rotation decoupling) to data acquisition in an HSQC experiment causes broadband homonuclear decoupling, giving a single signal for each proton chemical shift. This pure shift method improves both resolution and signal-to-noise ratio, without the need for special data processing.

AB - BIRD's eye view: Adding periodic BIRD J-refocusing (BIRD=bilinear rotation decoupling) to data acquisition in an HSQC experiment causes broadband homonuclear decoupling, giving a single signal for each proton chemical shift. This pure shift method improves both resolution and signal-to-noise ratio, without the need for special data processing.

KW - bilinear rotation decoupling

KW - gHSQC

KW - homonuclear decoupling

KW - NMR spectroscopy

KW - structure elucidation

U2 - 10.1002/anie.201305709

DO - 10.1002/anie.201305709

M3 - Journal article

C2 - 24014213

SN - 1433-7851

VL - 52

SP - 11616

EP - 11619

JO - Angewandte Chemie International Edition

JF - Angewandte Chemie International Edition

IS - 44

ER -