‘‘Perfecting’’ WATERGATE: clean proton NMR spectra from aqueous solution

Ralph W. Adams; Chloe M. Holroyd; Juan A. Aguilar; Lars Mathias Nilsson; Gareth A. Morris

doi:10.1039/c2cc37579f

‘‘Perfecting’’ WATERGATE: clean proton NMR spectra from aqueous solution

Ralph W. Adams, Chloe M. Holroyd, Juan A. Aguilar, Lars Mathias Nilsson, Gareth A. Morris

Food Analytics and Biotechnology

63 Citationer (Scopus)

3 Downloads (Pure)

Abstract

A simple modification of the WATERGATE solvent suppression method greatly improves the quality of ¹H NMR spectra obtainable from samples in H₂O. The new method allows ¹H signals to be measured even when close in chemical shift to the signal of water, as for example in the NMR spectra of carbohydrates.

Originalsprog	Engelsk
Tidsskrift	Chemical Communications
Vol/bind	49
Udgave nummer	4
Sider (fra-til)	358-360
Antal sider	3
ISSN	1359-7345
DOI	https://doi.org/10.1039/c2cc37579f
Status	Udgivet - 2013

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10.1039/c2cc37579f

“Perfecting” WATERGATE: clean proton NMR spectra from aqueous solutionForlagets udgivne version, 1,03 MB

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abstract = "A simple modification of the WATERGATE solvent suppression method greatly improves the quality of 1H NMR spectra obtainable from samples in H2O. The new method allows 1H signals to be measured even when close in chemical shift to the signal of water, as for example in the NMR spectra of carbohydrates.",

author = "Adams, {Ralph W.} and Holroyd, {Chloe M.} and Aguilar, {Juan A.} and Nilsson, {Lars Mathias} and Morris, {Gareth A.}",

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AU - Nilsson, Lars Mathias

AU - Morris, Gareth A.

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AB - A simple modification of the WATERGATE solvent suppression method greatly improves the quality of 1H NMR spectra obtainable from samples in H2O. The new method allows 1H signals to be measured even when close in chemical shift to the signal of water, as for example in the NMR spectra of carbohydrates.

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DO - 10.1039/c2cc37579f

M3 - Journal article

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VL - 49

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JO - Chemical Communications

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‘‘Perfecting’’ WATERGATE: clean proton NMR spectra from aqueous solution

Abstract

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